Effect of multi-ions doping on the properties of carbonated hydroxyapatite bioceramic

Safarzadeh, Marjan and Ramesh, Singh and Tan, Chou Yong and Chandran, Hari and Noor, Ahmad Fauzi Mohd and Krishnasamy, Sivakumar and Alengaram, Ubagaram Johnson and Ramesh, Subramaniam (2019) Effect of multi-ions doping on the properties of carbonated hydroxyapatite bioceramic. Ceramics International, 45 (3). pp. 3473-3477. ISSN 0272-8842, DOI https://doi.org/10.1016/j.ceramint.2018.11.003.

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Official URL: https://doi.org/10.1016/j.ceramint.2018.11.003


The effect of multi-ions (Mg2+, SiO4 4-, Zn2+, Cu2+) doping on the properties of carbonated hydroxyapatite (CHA) prepared by a wet chemical method has been investigated. Different combinations of ions were doped into the CHA and the as-synthesized compacts were sintered at 900 °C prior to body characterization. It was found that regardless of ions doping, the lattice structure of the CHA was not disrupted. In addition, secondary phases were not detected for all the multi-ions doped samples. The XRD and FTIR results further confirmed the presences of a B-Type CHA in the sintered samples. The XRD analysis revealed that the lattice parameters (c/a ratio) increased with dopant addition and resulted in a smaller crystallite size. The FESEM examination also showed the presences of smaller grain size for the multi-ions doped CHA samples thus indicating that the doping was beneficial in suppressing grain coarsening in carbonated hydroxyapatite.

Item Type: Article
Funders: Nippon Sheet Glass Foundation for Materials Science and Engineering Grant Number IF014-2017, PPP grant number PG207-2015A, FRG Grant Number FG011-17AFR
Uncontrolled Keywords: Carbonated hydroxyapatite; Multi-ions; Doping
Subjects: Q Science > QC Physics
R Medicine
T Technology > TA Engineering (General). Civil engineering (General)
T Technology > TJ Mechanical engineering and machinery
Divisions: Faculty of Engineering
Faculty of Medicine
Faculty of Science > Department of Physics
Depositing User: Ms. Juhaida Abd Rahim
Date Deposited: 15 Jan 2019 02:02
Last Modified: 15 Jan 2019 02:02
URI: http://eprints.um.edu.my/id/eprint/20000

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