Fracture strength and fractographic analysis of zirconia copings treated with four experimental silane primers

Mustafa, A.A. and Matinlinna, J.P. and Choi, A.H. and Razak, A.A.A. (2013) Fracture strength and fractographic analysis of zirconia copings treated with four experimental silane primers. Journal of Adhesion Science and Technology, 27 (1). pp. 68-80. ISSN 0169-4243, DOI https://doi.org/10.1080/01694243.2012.701507.

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Abstract

This study evaluated and compared the effect of new four experimental silane coupling agents on the fracture strength of zirconia copings. The findings were supported with fractographic and finite element analyses. All together 125 zirconia copings with a ?wall thickness of 0.6mm were fabricated on identical nickel-chromium master dies and then divided randomly into five groups (n=25). Four test groups were prepared according the experimental silane primer (labeled: OIWA1, OIWA2, OIWA3 and OIWA4) ?and one control group without silanization. The silane monomers used were: ?3-methacryloxypropyltrimethoxysilane (in OIWA1), ?3-acryloxypropyltrimethoxysilane (in OIWA2), ?3-?isocyanatopropyltriethoxysilane (in OIWA3) and styrylethyltrimethoxysilane (in OIWA4). Tribochemical sandblasting (silica-coating) treatment was performed to the inner surface of the copings in the ?test groups. All the specimens were silanized at the inner surfaces of the zirconia copings. Self-?adhesive universal resin cement was used to cement the copings to ?the underlying master die. Zirconia copings were vertically loaded on the ?cusp ?area until the first crack failure was occurred using Precision Universal Tester ?at a ?constant crosshead speed of 1mm/min. Then, the machine ?was manually controlled to cause more failure ?to further determine the texture of fracture. Three dimensional finite element analysis and fractography were performed to support the fracture strength findings. Based on the finite element analysis results, zirconia silanized with ?3-acryloyloxypropyltrimethoxysilane showed the highest fracture strength with a mean of ?963.75?N (SD 4.5N), while zirconia copings silanized with ?3-methacryloyloxypropyltrimethoxysilane showed a mean fracture strength value of ?925.65N (SD 2.4N). Styrylethyltrimethoxysilane-silanised zirconia showed mean fracture strength of 895.95N (SD 3.5N). Adding silane coupling agents to the resin-zirconia interface increased the fracture strengths significantly (ANOVA, p<0.05). Silanization with four new experimental silane primers in vitro produced significantly ?greater fracture strength than the control group not treated with the test silane.?

Item Type: Article
Funders: UNSPECIFIED
Additional Information: ISI Document Delivery No.: 093JJ Times Cited: 0 Cited Reference Count: 41 Cited References: Aboushelib MN, 2008, DENT MATER, V24, P1268, DOI 10.1016/j.dental.2008.02.010 Aboushelib MN, 2009, DENT MATER, V25, P989, DOI 10.1016/j.dental.2009.02.011 Amaral R, 2006, DENT MATER, V22, P283, DOI 10.1016/j.dental.2005.04.021 Attia A, 2011, J APPL ORAL SCI, V19, P388 Chen L, 2011, AM J DENT, V24, P79 Cho HY, 2011, PROCEDIA ENGINEER, V10, P1561, DOI 10.1016/j.proeng.2011.04.261 Derand T, 2008, Eur J Prosthodont Restor Dent, V16, P35 Heikkinen TT, 2009, SILICON-NETH, V1, P199, DOI 10.1007/s12633-009-9022-2 Heikkinen TT, 2007, ACTA ODONTOL SCAND, V65, P241, DOI 10.1080/00016350701459753 Ho GW, 2011, SILICON-NETH, V3, P117, DOI 10.1007/s12633-011-9079-6 Hooshmand T, 2004, DENT MATER, V20, P635, DOI 10.1016/j.dental.2003.08.005 Hooshmand T, 2002, DENT MATER, V18, P179, DOI 10.1016/S0109-5641(01)00047-1 Jang GW, 2011, PROCEDIA ENGINEER, V10, P1556, DOI 10.1016/j.proeng.2011.04.260 Johansson OK, 1967, J COMPOS MATER, V1, P278 Kern M, 1993, Dent Mater, V9, P151 Kern M, 2009, J ADHES SCI TECHNOL, V23, P1097, DOI 10.1163/156856109X432721 Kitayama S, 2009, DENT MATER J, V28, P446 Kitayama S, 2010, BIO-MED MATER ENG, V20, P77, DOI 10.3233/BME-2010-0617 Lin J, 2010, INT J ORAL SCI, V2, P24 Lin J, 2010, INT J ORAL SCI, V2, P28, DOI 10.4248/IJOS10002 Liu D, 2012, J ADHES SCI TECHNOL, V26, P1249, DOI 10.1163/156856111X593586 Lu YC, 2001, J ORAL REHABIL, V28, P805, DOI 10.1046/j.1365-2842.2001.00735.x Lung CYK, 2010, APPL SURF SCI, V257, P1228, DOI 10.1016/j.apsusc.2010.08.029 Matinlinna JP, 2004, INT J PROSTHODONT, V17, P155 Matinlinna Jukka P, 2007, J Contemp Dent Pract, V8, P1 Matinlinna JP, 2007, ACTA ODONTOL SCAND, V65, P44, DOI 10.1080/00016350600973060 Matinlinna JP, 2011, DENT MATER, V27, P273, DOI 10.1016/j.dental.2010.11.002 Matinlinna JP, 2007, DENT MATER, V23, P1173, DOI 10.1016/j.dental.2006.06.052 Matinlinna JP, 2006, J DENT, V34, P721, DOI 10.1016/j.jdent.2006.01.005 Matinlinna JP, 2006, J DENT, V34, P740, DOI 10.1016/j.jdent.2006.01.008 Matinlinna JP, 2006, DENT MATER, V22, P824, DOI 10.1016/j.dental.2005.11.035 Ozcan M, 2011, ODONTOLOGY, V99, P62, DOI 10.1007/s10266-010-0144-1 Ozcan M, 2003, DENT MATER, V19, P825 Piascik JR, 2009, DENT MATER, V25, P1116, DOI 10.1016/j.dental.2009.03.008 Sato H, 2008, DENT MATER J, V27, P408 Tanaka R, 2008, J DENT RES, V87, P666 Tsalouchou E, 2008, DENT MATER, V24, P308, DOI 10.1016/j.dental.2007.05.011 Tsukakoshi M, 2008, DENT MATER J, V27, P159 van Ooij WJ, 1998, CHEMTECH, V28, P26 Wilson KS, 2006, DENT MATER, V22, P995, DOI 10.1016/j.dental.2005.11.022 Xible AA, 2006, J PROSTHET DENT, V95, P224, DOI 10.1016/j.prosdent.2005.12.010 Mustafa, Ammar A. Matinlinna, Jukka Pekka Choi, Andy H. Razak, A. A. A. Research Management Center (RMC), International Islamic University Malaysia (IIUM) This study was financially supported by grants from Research Management Center (RMC), International Islamic University Malaysia (IIUM). The Center is highly acknowledged for this generous sponsorship. Taylor & francis ltd Abingdon
Uncontrolled Keywords: zirconia silane coupling agents tribochemical silica-coating fracture strength fractography finite element analysis silica-coated titanium dental ceramic crown bond strength coupling agents resin cement surface modification oxide ceramics luting cement adhesion insights
Subjects: R Medicine > RK Dentistry
Divisions: Faculty of Dentistry > Dept of Conservative Dentistry
Depositing User: Mr Ahmad Azwan Azman
Date Deposited: 17 Jul 2013 02:58
Last Modified: 21 Mar 2019 04:45
URI: http://eprints.um.edu.my/id/eprint/7741

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