Influence of fluoride phase on the tribological behaviour of Si3N4-SiC composites under extreme operating conditions

Mazumder, Subhrojyoti and Metselaar, Hendrik Simon Cornelis and Sukiman, Nazatul Liana and Mohd Zulkifli, Nurin Wahidah (2023) Influence of fluoride phase on the tribological behaviour of Si3N4-SiC composites under extreme operating conditions. Wear, 528-52. ISSN 0043-1648, DOI https://doi.org/10.1016/j.wear.2023.204970.

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Abstract

For extreme operating conditions such as high temperature and load, Si3N4-SiC composite is often used as wear resistant material. However, it suffers from a moderately high friction coefficient and wear rate at such working conditions; therefore, it is still an ongoing area of research for further development. This work strives to develop a state-of-the-art wear-resistant Si3N4 composite with SiC nanowire as reinforcement phase and MgF2 as an internal lubricating additive, particularly suitable for harsh operating conditions at both high temperatures and high loads. A significant improvement in tribological characteristics is observed when MgF2 is added into the composite matrix tested at 500 degrees C as compared to its parent Si3N4-SiC composite. When the load is increased from 6 to 14 N, the composite shows better wear resistance by forming a lubricious tribolayer at the contacting surface. Delamination is found to be the dominating wear mode for composites containing fluoride phase as identified by the morphological characterization of the worn surfaces. A comprehensive analysis of the evolution of different wear modes with respect to the variation in extreme operating conditions is articulated here.

Item Type: Article
Funders: Ministry of Education, Malaysia [Grant No: FRGS/1/2020/TK0/UM/02/12], Universiti Malaya, Malaysia [Grant No: GPF061A-2020]
Uncontrolled Keywords: Fluoride additives; Non-oxide ceramics; High temperature; High load; Wear characteristics
Subjects: T Technology > TJ Mechanical engineering and machinery
Divisions: Faculty of Engineering > Department of Mechanical Engineering
Depositing User: Ms. Juhaida Abd Rahim
Date Deposited: 08 Nov 2025 03:09
Last Modified: 08 Nov 2025 03:09
URI: http://eprints.um.edu.my/id/eprint/49781

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