Yeo, C.I. and Tiekink, E.R. (2011) 1,3-Bis(2-chloro-phen-yl)thio-urea: a monoclinic polymorph. Acta Crystallographica Section E: Structure Reports Online, 67 (pt11). ISSN 1600-5368, DOI PMID: 22219989.
![[img]](http://eprints.um.edu.my/style/images/fileicons/application_pdf.png)
|
PDF
26.pdf Download (355kB) |
Abstract
The title compound, C(13)H(10)Cl(2)N(2)S, represents a monoclinic polymorph of the previously reported ortho-rhom-bic form [Ramnathan et al. (1996 ▶). Acta Cryst. C52, 134-136]. The mol-ecule is twisted with the dihedral angle between the benzene rings being 55.37 (7)°. The N-H atoms are syn to each other, which contrasts their anti disposition in the ortho-rhom-bic form. In the crystal, mol-ecules assemble into zigzag chains along the c axis via N-H⋯S hydrogen bonds. Chains are connected into layers via C-H⋯Cl inter-actions, and these stack along the a axis.
| Item Type: | Article |
|---|---|
| Funders: | UNSPECIFIED |
| Additional Information: | Department of Chemistry, University of Malaya, 50603 Kuala Lumpur, Malaysia |
| Uncontrolled Keywords: | Chemistry |
| Subjects: | Q Science > QD Chemistry R Medicine |
| Divisions: | Faculty of Science > Department of Chemistry |
| Depositing User: | Mr. Faizal Hamzah |
| Date Deposited: | 03 Jul 2012 07:09 |
| Last Modified: | 30 Jan 2019 08:03 |
| URI: | http://eprints.um.edu.my/id/eprint/3464 |
Actions (login required)
 |
View Item |
