Synthesis of polycaprolactone using novel crude lipase: Parameter optimization

Thegarathah, Paveethra and Amran, Muhamad Harith and Jewaratnam, Jegalakshimi and Simarani, Khanom (2022) Synthesis of polycaprolactone using novel crude lipase: Parameter optimization. In: 6th Kuala Lumpur International Conference on Biomedical Engineering, BioMed 2021, 28-29 July 2021, Virtual, Online.

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Abstract

Polycaprolactone was synthesized using ring opening polymerization process by utilizing a novel lipase enzyme from Aspergillus niger sp. D-optimal design in DoE was used to optimize the reaction parameters for the synthesis of polycaprolactone. The variables selected were temperature (30–70 °C), time (30–150 min), mixing speed (100–500 rpm) and enzyme volume (5–9 mL). The response variable chosen is the number average molecular weight, Mn. Experimental results obtained was used to explain the interactions between parameters and responses were analyzed and validated. The result shows a good agreement with a minimum error between the actual and predicted values as the error is only 2.35. © 2022, Springer Nature Switzerland AG.

Item Type: Conference or Workshop Item (Paper)
Funders: UNSPECIFIED
Uncontrolled Keywords: Lipase; Polycaprolactone; Polymerization
Subjects: Q Science > QH Natural history > QH301 Biology
T Technology > TA Engineering (General). Civil engineering (General)
T Technology > TP Chemical technology
Divisions: Faculty of Engineering > Department of Chemical Engineering
Faculty of Science > Institute of Biological Sciences
Depositing User: Ms. Juhaida Abd Rahim
Date Deposited: 30 May 2025 07:44
Last Modified: 30 May 2025 07:44
URI: http://eprints.um.edu.my/id/eprint/43437

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