Saccharin and tert-Butyl Nitrite: Cheap and Efficient Reagents for the Synthesis of 1,2,3-Benzotriazine-4-(3H)-ones from 2-Aminobenzamides under Metal-Free Conditions

Khaligh, Nader Ghaffari and Johan, Mohd Rafie and Juan, Joon Ching (2018) Saccharin and tert-Butyl Nitrite: Cheap and Efficient Reagents for the Synthesis of 1,2,3-Benzotriazine-4-(3H)-ones from 2-Aminobenzamides under Metal-Free Conditions. Australian Journal of Chemistry, 71 (3). pp. 186-189. ISSN 0004-9425

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Official URL: https://doi.org/10.1071/CH17590

Abstract

A mild and eco-friendly protocol for the synthesis of 1,2,3-benzotriazine-4-(3H)-ones is described using saccharin as a cheap and efficient catalyst and tert-butyl nitrite as a diazotization reagent for the first time. The current method has advantages such as cost effectiveness, energy efficiency, and simple experimental procedure, good yield of the desired product, and metal-free and environmentally benign conditions.

Item Type: Article
Uncontrolled Keywords: Cost effectiveness; Energy efficiency; Sugars
Subjects: Q Science > QD Chemistry
T Technology > TA Engineering (General). Civil engineering (General)
Divisions: Deputy Vice Chancellor (Research & Innovation) Office > Nanotechnology & Catalysis Research Centre
Depositing User: Ms. Juhaida Abd Rahim
Date Deposited: 16 Jul 2019 08:23
Last Modified: 16 Jul 2019 08:23
URI: http://eprints.um.edu.my/id/eprint/21642

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