N-(1,5-Dimethyl-3-oxo-2-phenyl-2,3dihydro-1H-pyrazol-4-yl)acetamide-naph thalene-2,3-diol (1/1)

Asiri, A.M. and Khan, S.A. and Tan, K.W. and Ng, S.W. (2010) N-(1,5-Dimethyl-3-oxo-2-phenyl-2,3dihydro-1H-pyrazol-4-yl)acetamide-naph thalene-2,3-diol (1/1). Acta Crystallographica Section E: Structure Reports Online, 66 (7). O1850-U963. ISSN 1600-5368,

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In the reaction of naphthalene-2,3-diol and 4-aminoantipyrine in the presence of acetic acid, the amine function is acetylated and the resulting acetamide co-crystallizes with the diol in the title compound, C(13)H(15)N(3)O(2)center dot C(10)H(8)O(2), with 1:1 molar stoichiometry. The two components are linked by two O-H center dot center dot center dot O=C hydrogen bonds. One of the hydroxy groups interacts with the pyrazolone carbonyl O atom and the other hydroxy group interacts with the amide O atom of another component, generating a chain motif. Adjacent chains are linked into a layer motif via N-H center dot center dot center dot O interactions involving only the heterocyclic acetamide component.

Item Type: Article
Subjects: Q Science > Q Science (General)
Depositing User: Mr Faizal 2
Date Deposited: 12 Feb 2015 03:21
Last Modified: 31 Jan 2019 01:12
URI: http://eprints.um.edu.my/id/eprint/12715

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