1,5-Bis(2-oxoindolin-3-yl­­idene)thio­carbonohydrazide tetra­hydro­furan monosolvate

Pezeshkpour, Shaghayegh and Khaledi, Hamid and Ali, Hapipah Mohd (2012) 1,5-Bis(2-oxoindolin-3-yl­­idene)thio­carbonohydrazide tetra­hydro­furan monosolvate. Acta Crystallographica Section E: Structure Reports Online, 68 (Pt. 6). o1870. ISSN 1600-5368, DOI https://doi.org/10.1107/S1600536812022714.

1,5-Bis(2-oxoindolin-3-ylidene)thiocarbonohydrazide.pdf - Published Version

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Official URL: https://doi.org/10.1107/S1600536812022714


In the thio­carbonohydrazide mol­ecule of the title compound, C17H12N6O2S·C4H8O, the terminal indolin-2-one ring systems make a dihedral angle of 20.13 (6)° with each other. Two intra­molecular N—H⋯O hydrogen bonds are present, each of which generates an S(6) ring. In the crystal, N—H⋯O hydrogen bonds lead to a mol­ecular chain running along the b axis. The tetra­hydro­furan solvent mol­ecule is disordered over two orientations in a 0.561 (11):0.439 (11) ratio.

Item Type: Article
Uncontrolled Keywords: single-crystal X-ray study; T = 296 K; mean σ(C–C) = 0.002 A°; disorder in solvent or counterion; R factor = 0.040; wR factor = 0.121; data-toparameter ratio = 13.2.
Subjects: Q Science > Q Science (General)
Q Science > QD Chemistry
Divisions: Faculty of Science > Department of Chemistry
Depositing User: Ms. Jamilah Salleh
Date Deposited: 16 Jun 2014 09:00
Last Modified: 27 Nov 2019 06:48
URI: http://eprints.um.edu.my/id/eprint/10592

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