Synthesis and control of the morphology of SnO2 nanoparticles via various concentrations of Tinospora cordifolia stem extract and reduction methods

Fatimah, Is and Purwiandono, Gani and Jauhari, Muhammad Husnu and Maharani, Annabel Audita Aisyah Putri and Sagadevan, Suresh and Oh, Won-Chun and Doong, Ruey-an (2022) Synthesis and control of the morphology of SnO2 nanoparticles via various concentrations of Tinospora cordifolia stem extract and reduction methods. ARABIAN JOURNAL OF CHEMISTRY, 15 (4). ISSN 1878-5352, DOI https://doi.org/10.1016/j.arabjc.2022.103738.

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Abstract

SnO2 nanoparticles were synthesized utilizing Tinospora cordifolia stem extract. The effects of the concentration of the extract and the utilization of ultrasound irradiation on different chemical properties, mainly surface morphology, were studied. To determine the instrumental characteristics, X-ray diffraction, Fourier-Transform-Infra Red, scanning electron microscopy, and transmission electron microscope analyses were used. The optical properties of the material were studied using ultraviolet UV-visible diffuse reflectance spectrophotometry and photocatalytic activity tests on rhodamine B photodegradation. The results summarized the effect of T. cordifolia stem extract on the nucleation process during SnO2 crystallization, as a higher concentration leads to polymorphic forms with a greater particle size and an additional SnO phase. In addition, ultrasound-assisted reduction tended to produce a smaller particle size. The optical properties were found to be correlated with the particle size, as the higher particle size gave a smaller band gap energy and less photocatalytic activity for rhodamine B degradation.(c) 2022 The Author(s). Published by Elsevier B.V. on behalf of King Saud University. This is an open access article under the CC BY-NC-ND license (http://creativecommons.org/licenses/by-nc-nd/4.0/).

Item Type: Article
Funders: None
Uncontrolled Keywords: SnO (2 )nanoparticles; Photocatalyst; Photocatalysis; SnO2 nanoparticles; Nanorods
Subjects: Q Science > QC Physics
Divisions: Faculty of Science > Department of Physics
Depositing User: Ms. Juhaida Abd Rahim
Date Deposited: 04 Oct 2023 02:20
Last Modified: 04 Oct 2023 02:23
URI: http://eprints.um.edu.my/id/eprint/43039

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