Arman, H.D. and Miller, T. and Poplaukhin, P. and Tiekink, E.R.T. (2010) 2,2 `-(Disulfanediyl)dibenzoic acid-N,N `-bis(4-pyridylmethyl)ethanedithioamide (1/1). Acta Crystallographica Section E: Structure Reports Online, 66 (10). O2592-U742. ISSN 1600-5368,
Full text not available from this repository.Abstract
The asymmetric unit of the title co-crystal, C(14)H(14)N(4)S(2)center dot C(14)H(10)O(4)S(2), comprises a twisted 2,2'-(disulfanediyl)dibenzoic acid molecule [ dihedral angle between the benzene rings = 83.53 (14)degrees] and a U-shaped molecule of N,N'-bis(4-pyridylmethyl) ethanedithioamide in which intramolecular N-H center dot center dot center dot S hydrogen bonds are observed. Two molecules of each form a centrosymmetric ring, with an extended chair conformation, mediated by carboxyl-pyridine O-H center dot center dot center dot N hydrogen bonds between the carboxylic acid groups of two 2,2'-(disulfanediyl) dibenzoic acid molecules and pyridine-N atoms of two N, N'-bis(4-pyridylmethyl) ethanedithioamide molecules. The tetrameric aggregates are linked into a supramolecular chain along the b axis via amide-carbonyl N-H center dot center dot center dot O hydrogen bonds.
| Item Type: | Article |
|---|---|
| Funders: | UNSPECIFIED |
| Subjects: | Q Science > Q Science (General) |
| Depositing User: | Mr Faizal 2 |
| Date Deposited: | 19 Jan 2015 03:42 |
| Last Modified: | 31 Jan 2019 01:09 |
| URI: | http://eprints.um.edu.my/id/eprint/12211 |
Actions (login required)
 |
View Item |
