Pezeshkpour, Shaghayegh and Khaledi, Hamid and Ali, Hapipah Mohd (2012) 1,5-Bis(2-oxoindolin-3-ylidene)thiocarbonohydrazide tetrahydrofuran monosolvate. Acta Crystallographica Section E: Structure Reports Online, 68 (Pt. 6). o1870. ISSN 1600-5368, DOI https://doi.org/10.1107/S1600536812022714.
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Abstract
In the thiocarbonohydrazide molecule of the title compound, C17H12N6O2S·C4H8O, the terminal indolin-2-one ring systems make a dihedral angle of 20.13 (6)° with each other. Two intramolecular N—H⋯O hydrogen bonds are present, each of which generates an S(6) ring. In the crystal, N—H⋯O hydrogen bonds lead to a molecular chain running along the b axis. The tetrahydrofuran solvent molecule is disordered over two orientations in a 0.561 (11):0.439 (11) ratio.
| Item Type: | Article |
|---|---|
| Funders: | UNSPECIFIED |
| Uncontrolled Keywords: | single-crystal X-ray study; T = 296 K; mean σ(C–C) = 0.002 A°; disorder in solvent or counterion; R factor = 0.040; wR factor = 0.121; data-toparameter ratio = 13.2. |
| Subjects: | Q Science > Q Science (General) Q Science > QD Chemistry |
| Divisions: | Faculty of Science > Department of Chemistry |
| Depositing User: | Ms. Jamilah Salleh |
| Date Deposited: | 16 Jun 2014 09:00 |
| Last Modified: | 27 Nov 2019 06:48 |
| URI: | http://eprints.um.edu.my/id/eprint/10592 |
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